1-(3-Chloropropyl)-pyrrolidine → 4-Azoniaspiro[3,4]octane chloride
反応式
[Cl:1][CH2:2][CH2:3][CH2:4][N:5]1[CH2:9][CH2:8][CH2:7][CH2:6]1>O>[Cl-:1].[CH2:2]1[N+:5]2([CH2:9][CH2:8][CH2:7][CH2:6]2)[CH2:4][CH2:3]1参加物
3
反応条件
- 温度
- 20 °C
実験手順
An aqueous solution of 4-azoniaspiro[3,4]octane chloride was prepared by adding 1-(3-Chloropropyl)pyrrolidine (128 ml) to water (100 ml) at 94° C. over 25 minutes. The mixture was stirred for a further 5 minutes to give a clear yellow solution. This was cooled to 20° C. and stored in a bottle. Line washes of water (2×25 ml) were applied.
後処理
- customto give a clear yellow solution
出典と根拠
- ORDレコード
- ord-52e20117fb174a84b183fb621f670bc7
- 出典データセット
- uspto-grants-2010_12
- 特許番号
- US07851623B2
反応ノート
読み込み中…