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4-Methoxy-N-(4-methoxyphenyl)benzylamine → N-[(4-methoxyphenyl)methyl]-N-(4-methoxyphenyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxy-N-(4-methoxyphenyl)benzylamine | HCID 4131497 | — |
| 反応物 | 7-Methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid | HCID 13277484 | — |
| 生成物 | N-[(4-methoxyphenyl)methyl]-N-(4-methoxyphenyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxamide | HCID 59597406 | 46.1% |
反応手順
By the reaction and treatment in the same manner as in Example 1 using 7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid (1.5 g) and [(4-methoxyphenyl)methyl](4-methoxyphenyl)amine (0.88 g) as starting materials, N-[(4-methoxyphenyl)methyl]-N-(4-methoxyphenyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxamide (0.72 g) was obtained. melting point: 89-90° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07855297B2 |
| 出典データセット | uspto-grants-2010_12 |
| ORD ID | ord-bd78e0e7d19b4fd081a1a52c86c77f33 |
| 出典メモ | uspto-grants-2010_12 |