Hydrochloric Acid → HCID 66841583、化合物
反応式
C(OC(=O)[NH:7][CH:8]1[CH2:13][CH2:12][N:11]([CH2:14][C@H:15]2[C@@H:24]3[N:19]([CH2:20][CH2:21][CH2:22][CH2:23]3)[CH2:18][CH2:17][CH2:16]2)[CH2:10][CH2:9]1)(C)(C)C.[ClH:26]>O1CCOCC1>[ClH:26].[ClH:26].[ClH:26].[C@H:15]1([CH2:14][N:11]2[CH2:12][CH2:13][CH:8]([NH2:7])[CH2:9][CH2:10]2)[C@@H:24]2[N:19]([CH2:20][CH2:21][CH2:22][CH2:23]2)[CH2:18][CH2:17][CH2:16]1参加物
4
実験手順
The ester 62 (3.8 g, 10.8 mmol) is dissolved in 15 ml of dioxane and after addition of 70 ml of a 4M solution of HCl in dn of HCl in dioxan the mixture is stirred for 4 hours at RT. The product is filtered off and is used in the next step without further purification.
後処理
- filtrationThe product is filtered off
- customis used in the next step without further purification
出典と根拠
- ORDレコード
- ord-edf42419578243e3af85b8d9ebf9fc76
- 出典データセット
- uspto-grants-2010_12
- 特許番号
- US07858781B2
反応ノート
読み込み中…