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Sodium Cyanide → 2-(Hydroxyimino)-3-methoxy-3-methylbutanenitrile

HRID 2268105
ノート
印刷プレビュー

反応式

HRID 2268105 の反応式
[CH3:1][O:2][C:3]([CH3:8])([CH3:7])[CH:4]=[N:5][OH:6].ClCl.[C-:11]#[N:12].[Na+]>CCOCC.CO.O>[CH3:1][O:2][C:3]([CH3:8])([CH3:7])[C:4](=[N:5][OH:6])[C:11]#[N:12]
参加物実験手順後処理出典と根拠反応ノート

参加物

6

反応物 3

HCID 8929Sodium CyanideHCID 24526ChlorineHCID 86181628HCID 86181628、化合物

生成物 1

HCID 714138832-(Hydroxyimino)-3-methoxy-3-methylbutanenitrile

試薬・触媒・溶媒 2

HCID 3283Diethyl Ether溶媒HCID 22242641Methanol--water (1/1)溶媒

実験手順

53.6 g (0.46 mol) of 2-methoxy-2-methylpropionaldehyde oxime in ether (about 1 M) are initially taken at from −5 to −10° C. 35.8 g (0.5 mol) of chlorine gas are passed in, after which stirring is carried out for 1 hour at this temperature and the mixture is then evaporated down at 10° C. and the residue is taken up in diethyl ether. 24.7 g (0.5 mol) of sodium cyanide in 375 ml of 20:1 methanol/H2O are initially taken at 10° C. and the above ethereal solution is rapidly added dropwise. After 4 hours at room temperature, the mixture is filtered under suction and the residue is washed with twice 100 ml of methanol. The combined solutions are evaporated down and the residue is partitioned between methyl tert-butyl ether and water. Drying the organic phase over Na2SO4, evaporating down and crystallizing from dichloromethane/n-hexane give 41.1 g (63% of theory) of a white powder of melting point 102-104° C.

後処理

  1. customare initially taken at from −5 to −10° C
  2. customthe mixture is then evaporated down at 10° C.
  3. customare initially taken at 10° C.
  4. additionthe above ethereal solution is rapidly added dropwise
  5. waitAfter 4 hours at room temperature
  6. filtrationthe mixture is filtered under suction
  7. washthe residue is washed with twice 100 ml of methanol
  8. customThe combined solutions are evaporated down
  9. customthe residue is partitioned between methyl tert-butyl ether and water
  10. dry with materialDrying the organic phase over Na2SO4
  11. customevaporating down
  12. customcrystallizing from dichloromethane/n-hexane
  13. customgive 41.1 g (63% of theory) of a white powder of melting point 102-104° C.

出典と根拠

ORDレコード
ord-dd2f1de5dd544f3fae4031c29901a8a7
出典データセット
uspto-grants-2001_12
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06326399B1

反応ノート

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