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(3-Nitrophenyl)-thiophen-2-ylmethanone → N-[1-(3,4-Difluorophenyl)ethyl]-N-[(3-nitrophenyl)-(thiophen-2-yl)methyl}amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3-Nitrophenyl)-thiophen-2-ylmethanone | HCID 348407 | — |
| 反応物 | 1-(3,4-Difluorophenyl)ethanamine | HCID 3815974 | — |
| 生成物 | N-[1-(3,4-Difluorophenyl)ethyl]-N-[(3-nitrophenyl)-(thiophen-2-yl)methyl}amine | HCID 18347069 | 95% |
反応手順
Following a similar procedure to that described in Example (1a), 3.03 g of 3-nitrophenyl thiophen-2-yl ketone and 2.52 g of 1-(3,4-difluorophenyl)ethylamine were reacted, to obtain 4.62 g of the title compound as a reddish orange oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06329405B1 |
| 出典データセット | uspto-grants-2001_12 |
| ORD ID | ord-7247e6c2e9d94f76889dc03f811c4f4f |
| 出典メモ | uspto-grants-2001_12 |