3,3'-Dithiodipropionic acid → Disodium 3,3'-dithiobispropionate

HRID 2269537ノート

反応式

HRID 2269537 の反応式
C(=O)([O-])O.[Na+:5].[C:6]([OH:17])(=[O:16])[CH2:7][CH2:8][S:9][S:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14]>O>[C:6]([O-:17])(=[O:16])[CH2:7][CH2:8][S:9][S:10][CH2:11][CH2:12][C:13]([O-:15])=[O:14].[Na+:5].[Na+:5]

参加物

5

反応物 3

HCID 951163,3'-Dithiodipropionic acidHCID 516892Sodium BicarbonateHCID 178435178HCID 178435178、化合物

生成物 1

HCID 6454427Disodium 3,3'-dithiobispropionate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

A 1-liter polypropylene beaker was charged with a solution of 42 g (0.50 mole) of sodium hydrogen carbonate in 100 g of distilled water, followed by the slow addition of 52.5 g (0.25 mole) of 3,3′-dithiodipropionic acid, which required about 10 minutes. The resulting paste was spread on an evaporating tray and dried. The salt product was white-colored and melted above 225° C.

後処理

  1. customdried
  2. custommelted above 225° C.

出典と根拠

ORDレコード
ord-c0b0802a4a274e109a330d1de8d25fb9
出典データセット
uspto-grants-2001_12
特許番号
US06329455B1

反応ノート

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