化工社化工社 化学情報印刷レポート · 研究参考用
HCID 178500754、化合物 → 3-(3,4-Dimethyl-benzoyl)-7-methyl-1H-[1,8]naphthyridin-4-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | HCID 178500754 | HCID 178500754 | — |
| 溶媒 | Diphenyl Ether | HCID 7583 | — |
| 生成物 | 3-(3,4-Dimethyl-benzoyl)-7-methyl-1H-[1,8]naphthyridin-4-one | HCID 57754633 | 62% |
反応手順
Experimental conditions analogous to those described for Step 2 of Example 1 were used with 0.59 g (1.82 mmol) of 2-(3,4-Dimethyl-benzoyl)-3-(6-methyl-pyridin-2-ylamino)-acrylic acid methyl ester in 30 mL of diphenyl ether to yield 0.33 g of 3-(3,4-Dimethyl-benzoyl)-7-methyl-1H-[1,8]naphthyridin-4-one as a brown solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07557213B2 |
| 出典データセット | uspto-grants-2009_07 |
| ORD ID | ord-9d3b8fdd93c247c9b0a0ecd481dbd9bb |
| 出典メモ | uspto-grants-2009_07 |