cis-1,2,3,4,4a,5,6,10b-Octahydro-benzo[f]quinoline-8-carboxylic acid methyl ester → HCID 178497109、化合物
反応式
[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([OH:12])=O)=[CH:9][C:4]=2[N:3]=[CH:2]1.[CH3:13][O:14][C:15]([C:17]1[CH:30]=[CH:29][C:20]2[C@@H:21]3[C@H:26]([CH2:27][CH2:28][C:19]=2[CH:18]=1)[NH:25][CH2:24][CH2:23][CH2:22]3)=[O:16]>>[CH3:13][O:14][C:15]([C:17]1[CH:30]=[CH:29][C:20]2[C@@H:21]3[C@H:26]([CH2:27][CH2:28][C:19]=2[CH:18]=1)[N:25]([C:10]([C:8]1[CH:7]=[CH:6][C:5]2[NH:1][CH:2]=[N:3][C:4]=2[CH:9]=1)=[O:12])[CH2:24][CH2:23][CH2:22]3)=[O:16]参加物
3
実験手順
The title compound is prepared from 1H-benzoimidazole-5-carboxylic acid and cis-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline-8-carboxylic acid methyl ester following a procedure analogous to that described in Example 1. Yield: 92% of theory; LC (method 1): tR=2.57 min; Mass spectrum (ESI+): m/z=390 [M+H]+.
出典と根拠
- ORDレコード
- ord-b8afdae50a8349368829965a6bb40f54
- 出典データセット
- uspto-grants-2015_09