化工社化工社 化学情報印刷レポート · 研究参考用
Sodium aluminate → Sodium aluminosilicate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium aluminate | HCID 14766 | — |
| 反応物 | Sodium orthosilicate | HCID 26051 | — |
| 生成物 | Sodium aluminosilicate | HCID 72941443 | — |
反応手順
According to batch size, gel composition and contents of sodium silicate, sodium aluminate solution is prepared. This is added at a controlled rate and at ambient temperature to sodium silicate solution taken previously in a stainless steel reactor. Slurry of reaction mixture is allowed to crystallize at temperature 70-100° C. for 1 to 5 hours until Zeolite-A formation takes place. Zeolite-A slurry is filtered and washed till filtrate pH was ˜11 to 10.5. Wet cake thus obtained is dried in a dryer and dry powder was pulverized and subjected to analysis. The comparison of the properties of detergent builder Zeolite-A produced according to present invention (Example 10) and SASIL (Degussa-Henkel) is given in Table 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07560093B2 |
| 出典データセット | uspto-grants-2009_07 |
| ORD ID | ord-a7b91d1aa1754fbbaf6a75c47af75f06 |
| 出典メモ | uspto-grants-2009_07 |