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2-Amino-4,6-dimethyl pyrimidine → (5,7-Dimethyl-2-pyridin-2-yl-imidazo[1,2-a]-pyrimidin-3-yl)-(6-isocyanohexyl)amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4,6-dimethyl pyrimidine | HCID 13021 | — |
| 反応物 | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| 反応物 | 1,6-Diisocyanohexane | HCID 3391105 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | (5,7-Dimethyl-2-pyridin-2-yl-imidazo[1,2-a]-pyrimidin-3-yl)-(6-isocyanohexyl)amine | HCID 15521056 | — |
反応手順
Compound (2) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-4,6-dimethylpyrimidine solution (0.1 M, DCM), 0.575 ml of 1,6-diisocyanhexane solution (0.2 M, DCM), 0.500 ml of pyridine-2-carbaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-09d402d3ada54c4694616c3ca8d33b2a |
| 出典メモ | uspto-grants-2005_02 |