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1,1,3,3-Tetramethylbutyl isocyanide → [6,8-Dibromo-2-(2,3-dimethoxyphenyl)-5-methylimidazo[1,2-a]pyridin-3-yl]-(1,1,3,3-tetramethylbutyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| 反応物 | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| 反応物 | Wisteria sinensis, ext. | HCID 522994 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | [6,8-Dibromo-2-(2,3-dimethoxyphenyl)-5-methylimidazo[1,2-a]pyridin-3-yl]-(1,1,3,3-tetramethylbutyl)-amine | HCID 9829072 | — |
反応手順
Compound (6) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3,5-dibromo-6-methylpyridine solution (0.1 M, DCM), 0.575 ml of 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, DCM), 0.500 ml of 2,3-dimethoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-2162421c093a43f59d81760000eb9656 |
| 出典メモ | uspto-grants-2005_02 |