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Cyclohexyl isocyanide → [8-Benzyloxy-2-(3,5-dimethoxyphenyl)-imidazo[1,2-a]pyridin-3-yl]-cyclohexylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexyl isocyanide | HCID 79129 | — |
| 反応物 | 3,5-Dimethoxybenzaldehyde | HCID 81747 | — |
| 反応物 | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | [8-Benzyloxy-2-(3,5-dimethoxyphenyl)-imidazo[1,2-a]pyridin-3-yl]-cyclohexylamine | HCID 9911979 | — |
反応手順
Compound (10) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of cyclohexyl isocyanide solution (0.2 M, DCM), 0.500 ml of 3,5-dimethoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-989a97d5a8f2419da7256687cc0f15d0 |
| 出典メモ | uspto-grants-2005_02 |