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3-Hydroxybenzaldehyde → 3-[3-(2,6-Dimethylphenylamino)-6-nitroimidazo[1,2-a]pyridin-2-yl]-phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Hydroxybenzaldehyde | HCID 101 | — |
| 反応物 | 2,6-Dimethylphenyl isocyanide | HCID 76009 | — |
| 反応物 | 2-Amino-5-nitropyridine | HCID 77888 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | 3-[3-(2,6-Dimethylphenylamino)-6-nitroimidazo[1,2-a]pyridin-2-yl]-phenol | HCID 9864361 | — |
反応手順
Compound (12) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-5-nitropyridine solution (0.1 M, DCM), 0.575 ml of 2,6-dimethylphenyl isocyanide solution (0.2 M, DCM), 0.500 ml of 3-hydroxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-b197a4e0af4c4b9296dbdbdd21df01ff |
| 出典メモ | uspto-grants-2005_02 |