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2-Amino-4-methylpyridine → [2-(3,4-Dimethoxyphenyl)-7-methylimidazo[1,2-a]pyridin-3-yl]-(6-isocyanohexyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4-methylpyridine | HCID 1533 | — |
| 反応物 | Veratraldehyde | HCID 8419 | — |
| 反応物 | 1,6-Diisocyanohexane | HCID 3391105 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | [2-(3,4-Dimethoxyphenyl)-7-methylimidazo[1,2-a]pyridin-3-yl]-(6-isocyanohexyl)-amine | HCID 22591917 | — |
反応手順
Compound (24) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-4-methylpyridine solution (0.1 M, DCM), 0.575 ml of 1,6-diisocyanhexane solution (0.2 M, DCM), 0.500 ml of 3,4-dimethoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-69da732a5c2f44f58af76bcf57f85822 |
| 出典メモ | uspto-grants-2005_02 |