化工社化工社 化学情報印刷レポート · 研究参考用
Perchloric Acid → (8-Benzyloxy-2-cyclohexylimidazo[1,2-a]pyridin-3-ylamino)-acetic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Perchloric Acid | HCID 24247 | — |
| 反応物 | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| 反応物 | Methyl isocyanoacetate | HCID 547815 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | (8-Benzyloxy-2-cyclohexylimidazo[1,2-a]pyridin-3-ylamino)-acetic acid methyl ester | HCID 69732054 | — |
反応手順
Compound (30) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of methyl isocyanoacetate solution (0.2 M, DCM), 0.500 ml of cyclohexylcarbaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-f5bdd3d63b7542b3a523339961db6ca0 |
| 出典メモ | uspto-grants-2005_02 |