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2-Amino-6-methylpyridine → (5-Methyl-2-phenanthren-9-yl-imidazo[1,2-a]pyridin-3-yl)-(1,1,3,3-tetramethylbutyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-6-methylpyridine | HCID 15765 | — |
| 反応物 | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| 反応物 | Phenanthrene-9-carbaldehyde | HCID 78437 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | (5-Methyl-2-phenanthren-9-yl-imidazo[1,2-a]pyridin-3-yl)-(1,1,3,3-tetramethylbutyl)-amine | HCID 22591923 | — |
反応手順
Compound (36) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-6-methylpyridine solution (0.1 M, DCM), 0.575 ml of 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, DCM), 0.500 ml of phenanthrene-9-carbaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-dfda71c95a32446db74fee15f2c8a064 |
| 出典メモ | uspto-grants-2005_02 |