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2-Amino-4-methylpyrimidine → (2-Anthracen-9-yl-7-methylimidazo[1,2-a]pyrimidin-3-yl)-(1,1,3,3-tetramethylbutyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4-methylpyrimidine | HCID 7939 | — |
| 反応物 | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| 反応物 | 9-Anthracenecarboxaldehyde | HCID 69504 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | (2-Anthracen-9-yl-7-methylimidazo[1,2-a]pyrimidin-3-yl)-(1,1,3,3-tetramethylbutyl)-amine | HCID 22591919 | — |
反応手順
Compound (37) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-4-methylpyrimidine solution (0.1 M, DCM), 0.575 ml of 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, DCM), 0.500 ml of anthracene-9-carbaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849642B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-a619d9a795b8406cbc3a945dae2c5413 |
| 出典メモ | uspto-grants-2005_02 |