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Water → 2-(2-chloroacetyl)-6-pyridine carboxylic acid

HRID 2283520
ノート
印刷プレビュー

反応式

HRID 2283520 の反応式
[O:1]=[C:2]([C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([C:15]([O:17]C)=[O:16])[N:10]=1)[CH2:3]C(OCC)=O.O.S(Cl)([Cl:23])(=O)=O>C(OCC)(=O)C>[Cl:23][CH2:3][C:2]([C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([C:15]([OH:17])=[O:16])[N:10]=1)=[O:1]
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

5

反応物 3

HCID 962WaterHCID 24648Sulfuryl chlorideHCID 67071165HCID 67071165、化合物

生成物 1

HCID 116008662-(2-chloroacetyl)-6-pyridine carboxylic acid収率 85.1%

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒2 回

反応条件

温度
90 °C

実験手順

41.4 g of ethyl 3-oxo-3-(6-methoxycarbonyl-2-pyridyl)propionate was dissolved in a solution consisting of 42 ml of water and 414 ml of ethyl acetate, and the obtained solution was then cooled to a temperature between 5° C. and 10° C. Thereafter, a solution obtained by dissolving 35.6 g of sulfuryl chloride in 83 ml of ethyl acetate was added dropwise to the above cooled solution over approximately 30 minutes, while stirring. Thereafter, the obtained mixture was stirred at a temperature between 10° C. and 20° C. for 1 hour. Subsequently, the reaction solution was heated up to approximately 90° C., while the solvent was distilled away from the reaction solution. The reaction solution was continuously heated at a temperature between approximately 90° C. and 100° C. for 2 hours while stirring. Thereafter, the obtained mixed suspension (containing crystals) was cooled to approximately 10° C., and it was then stirred for 1 hour, followed by filtration, so as to obtain 27.99 g of 2-(2-chloroacetyl)-6-pyridine carboxylic acid in the form of yellow-brown crystals (melting point: 184° C. to 189° C.; purity: 98% to 99%).

後処理

  1. temperaturethe obtained solution was then cooled to a temperature between 5° C. and 10° C
  2. customThereafter, a solution obtained
  3. additionwas added dropwise to the above cooled solution over approximately 30 minutes
  4. stirringThereafter, the obtained mixture was stirred at a temperature between 10° C. and 20° C. for 1 hour
  5. distillationwas distilled away from the reaction solution
  6. temperatureThe reaction solution was continuously heated at a temperature between approximately 90° C. and 100° C. for 2 hours
  7. stirringwhile stirring
  8. additionThereafter, the obtained mixed
  9. additionsuspension (containing crystals)
  10. temperaturewas cooled to approximately 10° C.
  11. stirringit was then stirred for 1 hour
  12. filtrationfollowed by filtration

出典と根拠

ORDレコード
ord-de0105007b7042c7a31ef0ce98386e36
出典データセット
uspto-grants-2015_09
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US09145404B2

反応ノート

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