戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 2284298作成日:2026年10月27日

1-Methyl-1H-indole-5-carboxylic acid → N,N'-(Ethene-1,1-diylbis(4,1-phenylene))bis(1-methyl-1H-indole-5-carboxamide)

https://huagongshe.com/reaction/2284298

反応式

関与物質

役割名称HCID仕込み量
反応物1-Methyl-1H-indole-5-carboxylic acidHCID 7015601—
反応物4,4'-(Ethene-1,1-diyl)dianilineHCID 15471336—
生成物N,N'-(Ethene-1,1-diylbis(4,1-phenylene))bis(1-methyl-1H-indole-5-carboxamide)HCID 67688251—

反応手順

Compound 702 was prepared according to the procedure described in Scheme IV from 4,4′-(ethene-1,1-diyl)dianiline and 1-methylindole-5-carboxylic acid. 1H NMR (500 MHz, CDCl3) δ 8.20 (s, 2H), 7.93 (s, 2H), 7.79 (dd, J=1.7, 8.5 Hz, 2H), 7.66 (dd, J=1.7, 6.8 Hz, 4H), 7.42 (d, J=2.3 Hz, 2H), 7.39 (d, J=8.5 Hz, 4H), 7.15 (d, J=2.3 Hz, 2H), 6.61 (d, J=2.9 Hz, 2H), 5.44 (s, 2H), 3.86 (s, 6H).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09144557B2
出典データセットuspto-grants-2015_09
ORD IDord-1e571aa3798947cda293a6bbaabc495a
出典メモuspto-grants-2015_09