(3-Nitrophenyl)hydrazine → 2-(3-Nitrophenyl)-1-formylhydrazine

反応式

[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][NH2:11])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[N+](C1C=CC(NN[CH:23]=[O:24])=CC=1)([O-])=O>>[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][NH:11][CH:23]=[O:24])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]

参加物

反応物 2

HCID 3940977(3-Nitrophenyl)hydrazine

HCID 5008489Hydrazinecarboxaldehyde, 2-(4-nitrophenyl)-

生成物 1

HCID 205088472-(3-Nitrophenyl)-1-formylhydrazine

実験手順

By reacting 3-nitrophenylhydrazine as in the same manner as (1), 430 g of 2-(3-nitrophenyl)-1-formylhydrazine was obtained. Melting point: 168° to 169° C.

出典と根拠

ORDレコード: ord-aaa3f76ebc9f4d07a8151ff02646d72e
出典データセット: uspto-grants-1982_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04323643

反応ノート

読み込み中…