Stearic Acid → Lead stearate

HRID 2285695

反応式

HRID 2285695 の反応式
[C:1]([OH:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[Pb:21]=O.S(O)(O)(=O)=O.NO>>[C:1]([O-:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[Pb+2:21].[C:1]([O-:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

参加物

4

反応物 3

HCID 5281Stearic AcidHCID 14827Lead monoxideHCID 159255Hydroxylamine, sulfate (1:1)

生成物 1

HCID 61258Lead stearate

実験手順

A 500-ml capacity beaker was charged with 147 g of stearic acid and it was molten at 160°±5° C. in an oil bath under agitation by a glass vane, and 57.74 g of the lead monoxide powder (Sample A-6) and 0.31 g of powdery hydroxylamine sulfate were gradually added to the melt to effect reaction. Then, aging was conducted for 15 minutes to obtain a melt of lead stearate. The melt was poured into a watch glass and naturally cooled. The resulting solid was pulverized by an atomizer to obtain a lead stearate powder (Sample 2-7).

後処理

  1. additionwere gradually added to the melt
  2. customreaction

出典と根拠

ORDレコード
ord-0e5272dd73714e078e56e93879fbb9e4
出典データセット
uspto-grants-1982_04
特許番号
US04324768

関連ノート

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