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Diethyl Ether → HCID 12818620、化合物

HRID 2285821
ノート
印刷プレビュー

反応式

HRID 2285821 の反応式
[CH:1]1([NH:7][C:8]2[N:15]=[CH:14][CH:13]=[CH:12][C:9]=2[C:10]#[N:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C([CH:18]([C:22](Cl)=[O:23])[C:19](Cl)=[O:20])C.[CH2:25]([O:27]CC)[CH3:26]>>[CH2:25]([O:27][C:22]([C:18]1[C:19](=[O:20])[N:7]([CH:1]2[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]2)[C:8]2[C:9]([C:10]=1[NH2:11])=[CH:12][CH:13]=[CH:14][N:15]=2)=[O:23])[CH3:26]
参加物実験手順後処理出典と根拠反応ノート

参加物

4

反応物 3

HCID 3283Diethyl EtherHCID 109209242-Ethylpropanedioyl dichlorideHCID 128186532-(Cyclohexylamino)nicotinonitrile

生成物 1

HCID 12818620HCID 12818620、化合物

実験手順

To a solution of 20.1 g. (0.1 mole) of 2-cyclohexylaminonicotinonitrile in 1000 ml. of anhydrous ethyl ether was added 7.5 g. (0.05 mole) of ethyl malonyl chloride. The mixture was stirred at room temperature for 1 hour. The mixture was filtered and the filtrate was evaporated in a rotary evaporator. The residue was triturated with 30 ml. of ether and was filtered. The filtrate was evaporated and this residue was added to a solution of 2.3 g. (0.1 g. atom) of sodium in 250 ml. of ethanol. The mixture was stirred at room temperature for 5 minutes, diluted with water and was acidified with conc. hydrochloric acid. The solution was cooled in ice and the precipitate which formed was collected, air dried and was recrystallized twice from ethyl acetate to afford 1.0 g. of the title product, m.p. 172°-175° C.

後処理

  1. filtrationThe mixture was filtered
  2. customthe filtrate was evaporated in a rotary evaporator
  3. customThe residue was triturated with 30 ml
  4. filtrationof ether and was filtered
  5. customThe filtrate was evaporated
  6. additionthis residue was added to a solution of 2.3 g
  7. stirringThe mixture was stirred at room temperature for 5 minutes
  8. additiondiluted with water
  9. temperatureThe solution was cooled in ice
  10. customthe precipitate which formed
  11. customwas collected
  12. customair dried
  13. customwas recrystallized twice from ethyl acetate
  14. customto afford 1.0 g

出典と根拠

ORDレコード
ord-4eb27e84bdc541508558a91069573b6d
出典データセット
uspto-grants-1982_04
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04324893

反応ノート

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