Potassium Hydroxide → HCID 53885185、化合物
反応式
[CH3:1][O:2][N:3]=[C:4]([C:7]1[CH:12]=[N:11][CH:10]=[CH:9][N:8]=1)[C:5]#[N:6].[OH-:13].[K+]>CO.O>[CH3:1][O:2][N:3]=[C:4]([C:7]1[CH:12]=[N:11][CH:10]=[CH:9][N:8]=1)[C:5]([NH2:6])=[O:13]参加物
5
反応条件
- 温度
- 40 °C
実験手順
α-Methoxyiminopyrazineacetonitrile Z-isomer (6.0 g) was dissolved in 35 ml of methanol. A solution of potassium hydroxide (4 g) in 10 ml of water was added and the dark reaction mixture was stirred for 1 hour at a temperature of 40° C. The greater part of the methanol was evaporated under reduced pressure.
後処理
- customthe dark reaction mixture
- customThe greater part of the methanol was evaporated under reduced pressure
出典と根拠
- ORDレコード
- ord-dfbebaeb871d44c0b0049c0f3de67942
- 出典データセット
- uspto-grants-1982_04
- 特許番号
- US04327213
反応ノート
読み込み中…