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HRID 229049作成日:2026年10月24日

(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanol → (4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanone

https://huagongshe.com/ja/reaction/229049

反応式

関与物質

役割名称HCID仕込み量
反応物(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanolHCID 23078465—
触媒HCID 178418406HCID 178418406—
溶媒ChloroformHCID 6212—
生成物(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanoneHCID 2307852981.1%

反応手順

(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanol (1.17 g) was dissolved in chloroform (30 ml) to prepare a solution. Manganese dioxide (4.69 g) was added to the solution, and the mixture was stirred at room temperature overnight. The reaction solution was filtered through Celite, and the solvent was removed from the filtrate by distillation under the reduced pressure to give (4,5-dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanone (940 mg, yield 81%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07560558B2
出典データセットuspto-grants-2009_07
ORD IDord-d541dd2f8c2b40be824318bccb382ad9
出典メモuspto-grants-2009_07