関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Cyanuric chloride | HCID 7954 | — |
| 反応物 | Octyl p-aminobenzoate | HCID 26629 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 1,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine | HCID 20152733 | — |
反応手順
75 g of octyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water and then cooled to room temperature. The white crystals precipitated were filtered off under suction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04617390 |
|---|
| 出典データセット | uspto-grants-1986_10 |
|---|
| ORD ID | ord-406a8ee66c394100acc9d9181a37e888 |
|---|
| 出典メモ | uspto-grants-1986_10 |
|---|
