3-Decanone, 1-(3,4-dihydroxyphenyl)- → HCID 20230495、化合物

反応式

C([O:8][C:9]1[CH:14]=[CH:13][C:12]([CH:15]=[CH:16][C:17](=[O:24])[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])=[CH:11][C:10]=1[O:25][CH3:26])C1C=CC=CC=1.OC1C=C(CCC(=O)CCCCCCC)C=CC=1O>>[OH:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][CH:17]([OH:24])[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])=[CH:11][C:10]=1[O:25][CH3:26]

参加物

反応物 2

HCID 103781453-Decanone, 1-(3,4-dihydroxyphenyl)-

HCID 54185292HCID 54185292、化合物

生成物 1

HCID 20230495HCID 20230495、化合物収率 13.2%

実験手順

By following the same procedure as in Example 4 using 1.2 g of 1-(4-benzyloxy-3-methoxyphenyl)-1-nonen-3-one as a raw material, 660 mg of 1-(4-hydroxy-3-methoxyphenyl)-3-nonanone (a) as an oil and 120 mg of 1-(4-hydroxy-3-methoxyphenyl)-3-nonanol (b) as an oil were obtained.

出典と根拠

ORDレコード: ord-e735ee9959e34cde8936ef9c16816fc0
出典データセット: uspto-grants-1986_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04618627

反応ノート

読み込み中…