Methyl behenate → Potassium Behenate

HRID 2291517ノート

反応式

HRID 2291517 の反応式
[C:1]([O:24]C)(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[OH-].[K+:27]>CO>[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[K+:27]

参加物

4

反応物 2

HCID 13584Methyl behenateHCID 14797Potassium Hydroxide

生成物 1

HCID 23663647Potassium Behenate

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Methyl behenate (0.375 moles/mole of sucrose to be used in Step B) is saponified by stirring at reflux in methanol containing an equivalent amount of KOH. The reaction is stirred with heating until all methyl ester has been converted to soap as indicated by infrared analysis. The soap solution is used, as is in the next reaction step.

後処理

  1. stirringThe reaction is stirred
  2. customas is in the next reaction step

出典と根拠

ORDレコード
ord-0df2f8c266604a0898097b9e85e2ee78
出典データセット
uspto-grants-1989_01
特許番号
US04797300

反応ノート

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