N,N-Dimethylethylenediamine → HCID 86613123、化合物

HRID 229332

反応式

HRID 229332 の反応式
[C:1](#[N:10])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH3:11][C:12]1[NH:16][N:15]=[C:14]([NH2:17])[CH:13]=1.[CH3:18][N:19]([CH3:23])[CH2:20][CH2:21][NH2:22]>>[CH3:18][N:19]([CH3:23])[CH2:20][CH2:21][NH:22][C:3]1[CH:2]=[C:1]([NH:17][C:14]2[CH:13]=[C:12]([CH3:11])[NH:16][N:15]=2)[N:10]=[C:1]([CH:2]=[CH:3][C:4]2[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=2)[N:10]=1

参加物

4

反応物 3

HCID 66053N,N-DimethylethylenediamineHCID 746673-Phenylprop-2-enenitrileHCID 931461H-Pyrazol-3-amine, 5-methyl-

生成物 1

HCID 86613123HCID 86613123、化合物

実験手順

Example 66 was synthesized via Scheme 6 according to the general scheme provided above with the appropriate starting materials cinnamonitrile, 5-methyl-1H-pyrazole-3-amine, and N1,N1-dimethylethane-1,2-diamine. Structure of the target was confirmed by 1H-NMR. The 1H-NMR is attached.

後処理

  1. customExample 66 was synthesized via Scheme 6 according to the general scheme
  2. customprovided above with the

出典と根拠

ORDレコード
ord-b04a49fa52f34ea4892b4e5ad964f797
出典データセット
uspto-grants-2009_07
特許番号
US07563787B2

関連ノート

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