化工社化工社 化学情報印刷レポート · 研究参考用
Aluminium lithium hydride → 3-(8-Phenyloctyloxy)-2-hydroxypropylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aluminium lithium hydride | HCID 21226445 | — |
| 反応物 | 3-(8-Phenyloctyloxy)-2-hydroxypropylazide | HCID 21474713 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 3-(8-Phenyloctyloxy)-2-hydroxypropylamine | HCID 21474729 | 88.7% |
反応手順
A procedure similar to that described in Preparation 13 was repeated, except that 2.6 g of 3-(8-phenyloctyloxy)-2-hydroxypropylazide (Prepared as described in Preparation 65), 0.65 g of lithium aluminum hydride and 80 ml of anhydrous tetrahydrofuran were used, to give 2.11 g of the title compound, melting at 50° C. to 54° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05688823 |
| 出典データセット | uspto-grants-1997_11 |
| ORD ID | ord-28d42f0748f2475fa50735ed7cb36052 |
| 出典メモ | uspto-grants-1997_11 |