3-Tert-butyl-4-methoxybenzoyl chloride → Allyl 4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate

HRID 2294546

反応式

HRID 2294546 の反応式
[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8](Cl)=[O:9])([CH3:4])([CH3:3])[CH3:2].[OH:16][CH2:17][C:18]1[CH:29]=[CH:28][C:21]([C:22]([O:24][CH2:25][CH:26]=[CH2:27])=[O:23])=[CH:20][CH:19]=1>>[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8]([O:16][CH2:17][C:18]1[CH:19]=[CH:20][C:21]([C:22]([O:24][CH2:25][CH:26]=[CH2:27])=[O:23])=[CH:28][CH:29]=1)=[O:9])([CH3:4])([CH3:3])[CH3:2]

参加物

3

反応物 2

HCID 136335553-Tert-butyl-4-methoxybenzoyl chlorideHCID 22392687Allyl 4-hydroxymethylbenzoate

生成物 1

HCID 21474516Allyl 4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate

実験手順

In a manner similar to Example 1(d), by reaction of 2.4 g (18 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 1.9 g (10 mmol) of allyl 4-hydroxymethylbenzoate, 2.65 g (69%) of allyl ester are obtained in the form of a slightly yellow oil.

後処理

  1. customare obtained in the form of a slightly yellow oil

出典と根拠

ORDレコード
ord-ba9d3bf2603e4e80a5aecb363f30026e
出典データセット
uspto-grants-1997_11
特許番号
US05688817

関連ノート

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