関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1-Propanol | HCID 1031 | — |
| 反応物 | Ferulic Acid | HCID 445858 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | n-Propyl ferulate | HCID 9881169 | 64.3% |
反応手順
In a three-necked flask, 19.4 g (0.1 mole) of ferulic acid, 6.01 g (0.1 mole) of n-propyl alcohol, and 1.0 g of paratoluenesulfonic acid were placed, and 200 ml of benzene was added. This reaction mixture was stirred at 78° C. for 15 hours. Thereafter, the same procedures were taken as in Example 1 to obtain 15.2 g (yield: 64%) of n-propyl ferulate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05688991 |
|---|
| 出典データセット | uspto-grants-1997_11 |
|---|
| ORD ID | ord-cb2f8cf9927a4e25aade5ab629a20b25 |
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| 出典メモ | uspto-grants-1997_11 |
|---|
