化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → Aklomide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Benzoyl chloride, 2-chloro-4-nitro- | HCID 81522 | — |
| 生成物 | Aklomide | HCID 2075 | 90% |
反応手順
Thereafter, 2-chloro-4-nitrobenzoyl chloride (450 g, 2.1 m) was added dropwise to a stirred 28% ammonia solution (2,000 ml) at below room temperature between 9° and 16° C. The precipitated reaction mixture was washed with water and 30% methanol and then vacuum-dried to yield 2-chloro-4-nitrobenzamide (379 g, 90%, mp 168°-170° C.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04424371 |
| 出典データセット | uspto-grants-1984_01 |
| ORD ID | ord-9cec857d21fd40069e2cb33d97c7ca65 |
| 出典メモ | uspto-grants-1984_01 |