Cinnamoylbenzene → HCID 3798265、化合物
反応式
[CH:1](=[CH:8][C:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:17]1([NH:23][NH2:24])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(O)C>[C:17]1([N:23]2[CH:9]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)[CH:8]=[C:1]([C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=3)[NH:24]2)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1参加物
4
実験手順
20.8 g benzylideneacetophenone was condensed with 10.8 g phenylhydrazine in 400 ml boiling ethanol over 5 hours, and then allowed to cool. During the cooling process the desired reaction product separates. The sediment was filtered, washed with ethanol and dried.
後処理
- customover 5 hours
- temperatureto cool
- customreaction product
- filtrationThe sediment was filtered
- washwashed with ethanol
- customdried
出典と根拠
- ORDレコード
- ord-d52816a7584c405f995ea4670740be4f
- 出典データセット
- uspto-grants-1984_01
- 特許番号
- US04425179
反応ノート
読み込み中…