Ammonia → α-Phenyl-2-benzothiazolemethanamine

HRID 2295486ノート

反応式

HRID 2295486 の反応式
Cl.[NH2:2][CH:3]([C:10]1[S:11][C:12]2[CH:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1)[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.N>C(Cl)Cl>[NH2:2][CH:3]([C:10]1[S:11][C:12]2[CH:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1)[C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1

参加物

4

反応物 2

HCID 222AmmoniaHCID 23318519HCID 23318519、化合物

生成物 1

HCID 13342005α-Phenyl-2-benzothiazolemethanamine

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

The hydrochloride was dissolved with aqueous ammonia and methylene chloride, the aqueous layer was extracted with two portions of methylene chloride. The combined methylene chloride extracts were washed with brine, dried over Na2SO4, filtered and concentrated in vacuo. 13.1 g. of white solid of desired producted was obtained, mp. 68°-70° C.

後処理

  1. extractionthe aqueous layer was extracted with two portions of methylene chloride
  2. washThe combined methylene chloride extracts were washed with brine
  3. dry with materialdried over Na2SO4
  4. filtrationfiltered
  5. concentrationconcentrated in vacuo
  6. customof white solid of desired producted was obtained

出典と根拠

ORDレコード
ord-437c62e85e7d49d09e9685a0b2096388
出典データセット
uspto-grants-1984_01
特許番号
US04425338

反応ノート

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