Hydroxylamine → 5-Diethylphosphono-2-furaldehyde oxime
反応式
[CH2:1]([O:3][P:4]([C:9]1[O:13][C:12]([CH:14]=O)=[CH:11][CH:10]=1)([O:6][CH2:7][CH3:8])=[O:5])[CH3:2].[NH2:16][OH:17].C([O-])(=O)C.[Na+]>C(O)C>[CH2:1]([O:3][P:4]([C:9]1[O:13][C:12]([CH:14]=[N:16][OH:17])=[CH:11][CH:10]=1)([O:6][CH2:7][CH3:8])=[O:5])[CH3:2]参加物
5
実験手順
A solution of 5-diethylphosphono-2-furaldehyde (1 mmole) in ethanol was treated with hydroxylamine (1.1 mmole) and sodium acetate (2.2 mmole) at 25° C. for 12 h. Extraction and chromatography gave 5-diethylphosphono-2-furaldehyde oxime.
後処理
- extractionExtraction and chromatography
出典と根拠
- ORDレコード
- ord-b7621f5abcfd4a698bb94f5f29c14809
- 出典データセット
- uspto-grants-2002_12
- 特許番号
- US06489476B1
反応ノート
読み込み中…