1-(2,4-Dichlorophenyl)-2-(4-methylimidazol-2-yl)ethan-1-one → HCID 178430875、化合物

反応式

[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9](=[O:20])[C:10]([C:15]1C=CN[N:16]=1)=[CH:11][N:12]([CH3:14])[CH3:13].ClC1C=C(Cl)C=CC=1C(=O)CC1N[CH:33]=[C:34]([CH3:36])[N:35]=1>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9](=[O:20])[C:10]([C:15]1[NH:16][CH:33]=[C:34]([CH3:36])[N:35]=1)=[CH:11][N:12]([CH3:13])[CH3:14]

参加物

反応物 2

HCID 1784308761-(2,4-Dichlorophenyl)-2-(4-methylimidazol-2-yl)ethan-1-one

HCID 178483574HCID 178483574、化合物

生成物 1

HCID 178430875HCID 178430875、化合物

実験手順

Made using the same procedure as for 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-pyrazolylprop-2-en-1-one except that 1-(2,4-dichlorophenyl)-2-(4-methylimidazolyl)ethan-1-one (II, 1.0 g, 3.7 mmol) was used. The crude residue was used without purification.

後処理

customThe crude residue was used without purification

出典と根拠

ORDレコード: ord-75cfaaf948c34d09b5a6f74bd0129003
出典データセット: uspto-grants-2002_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06489344B1

反応ノート

読み込み中…

参加物