Benzyl Isothiocyanate → 4-({[4-benzyl-5-(thiophen-2-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}methyl)pyridine

HRID 229759

反応式

HRID 229759 の反応式
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([NH:8][NH2:9])=O.[CH2:10]([N:17]=[C:18]=[S:19])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.Br[CH2:21][C:22]1[CH:27]=[CH:26][N:25]=[CH:24][CH:23]=1>>[CH2:10]([N:17]1[C:6]([C:2]2[S:1][CH:5]=[CH:4][CH:3]=2)=[N:8][N:9]=[C:18]1[S:19][CH2:21][C:22]1[CH:27]=[CH:26][N:25]=[CH:24][CH:23]=1)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

参加物

4

反応物 3

HCID 2346Benzyl IsothiocyanateHCID 73098Thiophene-2-carbohydrazideHCID 6427994-(Bromomethyl)pyridine

生成物 1

HCID 112570494-({[4-benzyl-5-(thiophen-2-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}methyl)pyridine

実験手順

This compound was synthesized using the same methodology as described in Example 1 above, using 2-thiophencarboxylic acid hydrazide, benzyl isothiocyanate and 4-bromomethylpyridine as the starting materials. (M+H)+−365.

後処理

  1. customThis compound was synthesized

出典と根拠

ORDレコード
ord-bb2e844f03fc4d3a800ea521b1d67e00
出典データセット
uspto-grants-2009_07
特許番号
US07563905B2

関連ノート

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