関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2,5-Dianilinoterephthalic acid | HCID 82351 | — |
| 反応物 | 1,4-Benzenedicarboxylic acid, 2,5-bis[(4-methoxyphenyl)amino]- | HCID 3084837 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Quinacridone | HCID 13976 | — |
反応手順
A mixture (one part) of 2,5-dianilino-terephthalic acid (95%) and 2,5-dianisidino-terephthalic acid (5%) was dissolved in polyphosphoric acid (6.14 parts at 118.5%). The solution, already at 100° C., was heated to 133° C. for 3 hours, cooled and diluted. The solution was drowned into methanol (11.6 parts) and heated at 120° C. for 4 hours. A very bluish, transparent quinacridone pigment, dispersible in an automotive finish, was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06494949B2 |
|---|
| 出典データセット | uspto-grants-2002_12 |
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| ORD ID | ord-de17842ae26e4b99a747535771943f47 |
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| 出典メモ | uspto-grants-2002_12 |
|---|
