化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → Propylene Glycol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 反応物 | Propylene glycol methanol | HCID 86614669 | — |
| 溶媒 | Propylene Carbonate | HCID 7924 | — |
| 生成物 | Propylene Glycol | HCID 1030 | — |
| 生成物 | Dimethyl Carbonate | HCID 12021 | — |
反応手順
In a process as described in FIG. 1 7 t/h (tonnes per hour) propylene carbonate is fed into the upper part of a reactive distillation zone. Sodium methanolate in 0.5 t/h propylene glycol/methanol mixture as transesterification catalyst is also passed into the upper part of zone in an amount of 0.05 t/h. Twenty t/h methanol, fed into a lower part of the distillation zone, passes upward, and reacts with the propylene carbonate to form propylene glycol product and dimethyl carbonate. The propylene glycol is recovered in an amount of 5 t/h.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07563919B2 |
| 出典データセット | uspto-grants-2009_07 |
| ORD ID | ord-92e778977c1649e1ab96e2996ca52116 |
| 出典メモ | uspto-grants-2009_07 |