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Leucinamide hydrochloride → N-[N-(3,4-dichlorophenyl)-L-alanyl]-L-leucine amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Leucinamide hydrochloride | HCID 2733199 | — |
| 反応物 | 2-(3,4-Dichloro-phenylamino)-propionic Acid | HCID 6916426 | — |
| 生成物 | N-[N-(3,4-dichlorophenyl)-L-alanyl]-L-leucine amide | HCID 131721930 | — |
反応手順
Following General Procedure D and using L-leucinamide hydrochloride (Sigma) and N-(3,4-dichlorophenyl)-D,L-alanine (from Example A above), the title compound was prepared. This compound was then purified by column chromatography, eluted first with 1:1 EtOAc/hexane, then with 5% MeOH in methylene chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06495693B2 |
| 出典データセット | uspto-grants-2002_12 |
| ORD ID | ord-668fd6c6dc1c48f9a0e4a10c089d4849 |
| 出典メモ | uspto-grants-2002_12 |