Ethyl Acetate → 3,5-Dimethoxy-4-methyl-benzoic acid N-(1-tert-butyl-butyl)-N'-(2-ethyl-3-methoxy-benzoyl)-hydrazide
反応式
[C:1]([CH:5]([N:10]([C:23](=[O:35])[C:24]1[CH:29]=[C:28]([O:30][CH3:31])[C:27]([CH3:32])=[C:26]([O:33][CH3:34])[CH:25]=1)[NH:11][C:12](=[O:22])[C:13]1[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[C:14]=1[CH3:21])[CH2:6][CH2:7][CH2:8]C)([CH3:4])([CH3:3])[CH3:2].[C:36](OCC)(=O)C>CCCCCC>[C:1]([CH:5]([N:10]([C:23](=[O:35])[C:24]1[CH:25]=[C:26]([O:33][CH3:34])[C:27]([CH3:32])=[C:28]([O:30][CH3:31])[CH:29]=1)[NH:11][C:12](=[O:22])[C:13]1[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[C:14]=1[CH2:21][CH3:36])[CH2:6][CH2:7][CH3:8])([CH3:4])([CH3:3])[CH3:2]参加物
4
実験手順
RG-115852, 3,5-dimethoxy-4-methyl-benzoic acid N-(1-tert-butyl-pentyl)-N′-(3-methoxy-2-methyl-benzoyl)-hydrazide. 1H NMR (CDCl3, 500 MHz), δ (ppm): 7.05 (t, 1H), 7.0 (s, 1H), 6.85 (d, 1H), 6.65 (s, 2H), 6.25 (d, 1H), 4.7 (d, 1H), 3.89 (s, 3H), 3.78 (s, 6H), 2.10 (s, 3H), 1.86 (s, 3H), 1.3-1.6 (br m, 6H), 1.06, 0.99 (2s, 9H), 0.94 (t, 3H); TLC Rf=0.55 (1:1 ethyl acetate:hexane).