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Sodium borohydride → 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium borohydride | HCID 4311764 | — |
| 反応物 | 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzaldehyde | HCID 10829743 | — |
| 生成物 | 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol | HCID 57315820 | 93.9% |
反応手順
In substantially the same manner in Reference Example 93, 3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzaldehyde (6.47 g) was reduced by sodium borohydride (760 mg) to obtain 3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol (6.11 g, yield 93%) as crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06495581B1 |
| 出典データセット | uspto-grants-2002_12 |
| ORD ID | ord-d7ebf342acfc432abde65e22e5262aed |
| 出典メモ | uspto-grants-2002_12 |