化工社化工社 化学情報印刷レポート · 研究参考用
3,5-Difluorophenylacetic acid → HCID 178496843、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| 反応物 | HCID 22592446 | HCID 22592446 | — |
| 生成物 | HCID 178496843 | HCID 178496843 | — |
反応手順
Following General Procedure C above and using 3,5-difluorophenylacetic acid (Aldrich) and 1-tert-butoxycarbonyl-2-(1-aminoethyl)-4-methoxycarbonyl-4-phenyl-2-imidazoline (Example K), the title compound was prepared as a white foam (90%). The reaction was monitored by tlc (Rf=0.39 in 3:2 hexanes/EtOAc) and the product was purified by flash column chromatography.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849650B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-9c6f40ad374f4524be641c8c618468b0 |
| 出典メモ | uspto-grants-2005_02 |