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3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine Iso-butyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Dichloroaniline | HCID 7257 | — |
| 反応物 | Isobutyl pyruvate | HCID 83084 | — |
| 生成物 | N-(3,4-dichlorophenyl)alanine Iso-butyl Ester | HCID 15434840 | — |
反応手順
Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.55 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849650B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-6888b8e4ce4c4a608f80013bbcb300d7 |
| 出典メモ | uspto-grants-2005_02 |