戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 23028作成日：2026年10月25日

3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine isopropyl ester

https://huagongshe.com/reaction/23028

反応式

関与物質

役割名称HCID仕込み量
反応物3,4-DichloroanilineHCID 7257—
反応物Isopropyl pyruvateHCID 9964097—
生成物N-(3,4-dichlorophenyl)alanine isopropyl esterHCID 54285545—

反応手順

Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and isopropyl pyruvate (prepared by following General Procedure AO above using isopropanol in place of iso-butanol), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.4 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06849650B2
出典データセットuspto-grants-2005_02
ORD IDord-fdc87d00b5384ac88b4d61aa969f1d55
出典メモuspto-grants-2005_02