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HRID 23030作成日：2026年10月26日

3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine Methyl Ester

https://huagongshe.com/reaction/23030

反応式

関与物質

役割名称HCID仕込み量
反応物3,4-DichloroanilineHCID 7257—
反応物Methyl pyruvateHCID 11748—
生成物N-(3,4-dichlorophenyl)alanine Methyl EsterHCID 54289412—

反応手順

Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and methyl pyruvate (Aldrich), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.55 in 25% EtOAc/hexanes) and purification was by flash chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06849650B2
出典データセットuspto-grants-2005_02
ORD IDord-3665ec35c5b94971b7684d4f6339c117
出典メモuspto-grants-2005_02