反応式
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=O.[C:11]([NH:15][OH:16])([CH3:14])([CH3:13])[CH3:12]>>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=[N+:15]([C:11]([CH3:14])([CH3:13])[CH3:12])[O-:16]参加物
3
実験手順
The title compound was prepared according to the procedure described in Example 7 using 2-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.9% overall yield as white crystals, m.p. 109.1° C. (Rf=0.53 on a silica gel plate using ethyl acetate as the eluant).
後処理
- customThe title compound was prepared
出典と根拠
- ORDレコード
- ord-5e1cce7b983140e695bd0406630df580
- 出典データセット
- uspto-grants-2002_08
- 特許番号
- US06433008B1
関連ノート
読み込み中…