化工社化工社 化学情報印刷レポート · 研究参考用
Diallylamine → N,N-diallyl-3-chloropropaneamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diallylamine | HCID 31279 | — |
| 反応物 | 3-Chloropropionyl chloride | HCID 69364 | — |
| 生成物 | N,N-diallyl-3-chloropropaneamide | HCID 4688188 | — |
反応手順
comprises first reacting 3-chloropropionyl chloride (CPC) with diallylamine to form N,N-diallyl-3-chloropropaneamide, then reacting this product with RF-iodide followed by eliminating HCl and Hl by dehydrohalogenating with a base such as an alkali metal hydroxide. The product of the formula IIa is then washed with water followed by separating the aqueous layer.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06436235B1 |
| 出典データセット | uspto-grants-2002_08 |
| ORD ID | ord-65434ece63914fc586e3e3f61ef164e4 |
| 出典メモ | uspto-grants-2002_08 |