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2-Naphthylamine → 2-[N-(naphth-2-yl)amino]butanoic Acid Ethyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Naphthylamine | HCID 7057 | — |
| 反応物 | Butanoic acid, 2-bromo-, ethyl ester | HCID 79039 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | 2-[N-(naphth-2-yl)amino]butanoic Acid Ethyl Ester | HCID 10131322 | — |
反応手順
Following General Procedure AJ above and using 2-aminonaphthalene (Aldrich) and ethyl 2-bromobutyrate (Aldrich), the title compound was prepared as a solid, m.p. 81-83° C. The reaction was monitored by silica gel tlc (Rf=0.5 in CHCl3). Purification was by chromatography (silica gel using chloroform as the eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849650B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-6e4353b64d914f0d9dd8180a2a62c6ef |
| 出典メモ | uspto-grants-2005_02 |