化工社化工社 化学情報印刷レポート · 研究参考用
Isobutyl pyruvate → N-(2-methylquinolin-6-yl)alanine Iso-butyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutyl pyruvate | HCID 83084 | — |
| 反応物 | 2-Methylquinolin-6-amine | HCID 103148 | — |
| 生成物 | N-(2-methylquinolin-6-yl)alanine Iso-butyl Ester | HCID 54119157 | — |
反応手順
Following General Procedure AA above and using 6-amino-2-methylquinoline (Lancaster) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared. The reaction was monitored by silica gel tlc (Rf=0.44 in 50% EtOAc/hexanes). Purification was by flash chromatography (silica gel using 50% EtOAc/hexanes as the eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849650B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-e4defc8176564c78905f4f164eeb6e1d |
| 出典メモ | uspto-grants-2005_02 |